High Resolution NMR in the Solid State

Stejskal, E. O.; Memory, J. D.

ISBN 10: 0195073800 / ISBN 13: 9780195073805

Editore: Oxford University Press, 1994

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Codice articolo 9780195073805

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Titolo: High Resolution NMR in the Solid State

Casa editrice: Oxford University Press

Data di pubblicazione: 1994

Legatura: Rilegato

Condizione: Usado - bueno

Descrizione articolo

Riassunto:

This text was developed from a course for physical chemistry and chemical physics students using cross-polarization (CP) magic angle spinning (MAS) NMR in their laboratory assignments. The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin, high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in solution NMR. The student can observe the way interacting spin systems behave in the solid state, and have a quantum mechanically rigorous understanding of solid-state spin phenomena. The text will have the added benefit of serving as a self-study resource for students seeking to learn the underlying principles of laboratory experiments using the technique. The history of NMR is also treated, and the instrumentation of the spectrometer and probe are discussed.

Recensione:

To say that the appearance of a book on the fundamentals of CP/MAS is timely would be a gross understatement ... this is an excellent book and should be read carefully, and understood, by all practitioners of CP/MAS NMT spectroscopy. (Glenn Penner, University of Guelph, Magnetic Resonance in Chemistry, Vol. 33 989 (1995))