Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-based Approach - Brossura

Simpson, Jeffrey H.

Brossura

ISBN 10: 0120885220 ISBN 13: 9780120885220

Casa editrice: Academic Pr, 2008

Riassunto

This book contains 30-40 quality 2D NMR data sets following an introductory section describing the methodology employed. Many other books describe the methods used, but none offer a large number of problems. Instructors at universities and colleges at the present time are forced to cobble together problems from a wide range of sources. The fragmentary approach to assembling course materials has a negative impact on course continuity and thus adversely impacts student retention. This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty.

• Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra
• Contains 20 known and 20 unknown structure determination problems
• Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing.

Su questo libro

Informazioni sull?autore

Jeffrey H Simpson, PhD, was Director of the Instrumentation Facility in the Department of Chemistry at M.I.T. from 2006 to 2017. Dr. Simpson’s career in NMR/instrumentation research and instruction spans 20 years, and he has authored an introductory text on the subject of NMR as well as publishing a number of peer-reviewed articles. He is one of the Founding Members of the New England NMR Society and served as VP from its inception to 2017. He currently is a faculty member in the Department of Chemistry at the University of Richmond.

Dalla quarta di copertina

Ideal for advanced undergraduate and graduate courses in organic spectroscopy, this book provides the analytical skills and methodologies needed to assign nuclear magnetic resonances to known and unknown molecular structures. Part I covers the essential knowledge along with worked examples synthetic organic chemists should possess to understand and apply NMR in their research. Part II presents a comprehensive selection of 40 problems (20 knowns and 20 unknowns), consisting of 1H and 13C 1-D spectra plus multiple 2-D spectra.

While most books on the subject focus on mathematically rigorous treatments, this text balances rigor with guidance, providing novice and experienced chemists with the tools needed to understand and interpret 2-D NMR spectra.
? Optimizes workflow by presenting strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra
? Improves analytical and interpretation skills through the use of extensive examples and problem-solving techniques
? Enhances understanding through detailed explanations of key concepts, including an extensive glossary

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Dettagli dell'edizione

• Editore: Academic Pr
• Data di pubblicazione: 2008
• Lingua: Inglese
• ISBN 10: 0120885220
• ISBN 13: 9780120885220
• Rilegatura: Copertina flessibile
• Numero edizione: 1
• Numero di pagine: 362
• Contatto del produttore: Academic Press; https://shop.elsevier.com/; ; 230 PARK AVENUE, SUITE 800; NY; NY; 10169; U.S.A.
• Persona responsabile: non disponibile