Methods In Chemical Analysis, Originated Or Developed In The Kent Chemical Laboratory Of Yale University - Brossura

Gooch, Frank Austin

 
9780548805664: Methods In Chemical Analysis, Originated Or Developed In The Kent Chemical Laboratory Of Yale University

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METHODS IN CHEMICAL ANALYSIS ORIGINATED OR DEVELOPED IN THE KENT CHEMICAL LABORATORY OF YALE UNIVERSITY COMPILED - 1912 -- PREFATORY NOTE THE - object of this volume is to present concisely the principal results reached by workers in the Kent Chemical Laboratory of Yale University in the investigation and development of methods in chemical analysis. In the account of processes, modified or original, only proved procedure and immediately related experimental data are, as a rule, given. For further details in respect to the elaboration of processes, the discussion of difficulties, and the experimental illustration of the effects of varying the prescribed procedure, references are given to the original sources from which this summary has been compiled. To his colleagues, Professors Philip E. Browning, R. G. Van Name, and W. A. Drushel, the compiler is much indebted for valuable criticism of the proof sheets. CONTENTS. CHAPTER I. APPLIANCES AND GENERAL PROCEDURE. Mechanical Processes. - The determination of products gaseous at ordinary temperatures by loss of weight, I. The distillation and condensation of volatile products, 3. The distillation and absorption of volatile products, 4 apparatus with ground joints, 4 apparatus with sealed joints, 5. The removal of volatile products from material to be reserved for treatment. The prevention of mechanical loss from solution in reactions evolving gaseous products, 6. The transfer of liquids and gases under pressure, 7. A convenient form of rotary shaker, g. The purification of precipitates by solution and reprecipitation, 10. Electrolytic processes. - The rotating cathode, I I. The filtering crucible, 13 electrolysis and subsequent filtration, 13electrolysis with filtration, 16 electrolysis wit h continuous filtration, I 7. The fixation of chlorine on the silver anode, 20 hydrochloric acid, silver anode, and platinum cathode, 20 sodium chloride, silver anode, and mercury cathode, 22. Iodometric processes. - The standardizatio

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