Principles and Practice of Analytical Chemistry - Rilegato

Fifield, F. W.; Kealey, D.

Rilegato

ISBN 10: 0751402265 ISBN 13: 9780751402261

Casa editrice: Chapman & Hall, 1995

Riassunto

A text for both undergraduate and graduate students of analytical chemistry and industrial trainees, providing a basic understanding of the principles, instrumentation, and applications of chemical analysis as it is currently practiced. This edition pays substantial attention to significant advances in analytical instrumentation since the third edition of 1990, such as high-performance capillary electrophoresis as a separation technique and two-dimensional nuclear magnetic resonance spectroscopy as an aid to structural analysis, and revises aspects of atomic spectrometry. Annotation c. by Book News, Inc., Portland, Or.

Su questo libro

L'autore:

D. Kealey is Senior Lecturer in Analytical Chemistry and Director of Kingston Analytical Services in the School of Applied Chemistry at Kingston University.

Contenuti:

1 Introduction.- 2 The Assessment of Analytical Data.- 2.1 Definitions and basic concepts.- 2.2 The nature and origin of errors.- 2.3 The evaluation of results and methods.- 3 Ph, Complexation And Solubility Equilibria.- 3.1 Chemical reactions in solution.- 3.2 Solvents in analytical chemistry.- 3.3 Acid-base equilibria.- 3.4 Complexation equilibria.- 3.5 Solubility equilibria.- 4 Separation Techniques.- 4.1 Solvent extraction.- 4.2 Chromatography.- 4.3 Electrophoresis.- 5 Titrimetry and Gravimetry.- 5.1 Titrimetry.- 5.2 Gravimetry.- 6 Electrochemical Techniques.- 6.1 Potentiometry.- 6.2 Polarography, stripping voltammetry and amperometric techniques.- 6.3 Electrogravimetry and coulometry.- 6.4 Conductometric titrations.- 7 An Introduction to Analytical Spectrometry.- 8 Atomic Spectrometry.- 8.1 Arc/spark atomic (optical) emission spectrometry.- 8.2 Glow discharge atomic emission spectrometry.- 8.3 Plasma emission spectrometry.- 8.4 Inductively coupled plasma-mass spectrometry (ICP-MS).- 8.5 Flame emission spectrometry.- 8.6 Atomic absorption spectrometry.- 8.7 X-ray emission spectrometry.- 9 Molecular Spectrometry.- 9.1 Visible and ultraviolet spectrometry.- 9.2 Infrared spectrometry.- 9.3 Nuclear magnetic resonance spectrometry (nmr).- 9.4 Mass spectrometry.- 9.5 Spectrometric identification of organic compounds.- 10 Radiochemical Methods In Analysis.- 10.1 Nuclear structure and nuclear reactions.- 10.2 Instrumentation and measurement of radioactivity.- 10.3 Analytical uses of radionucleides.- 11 Thermal Techniques.- 11.1 Thermogravimetry.- 11.2 Differential thermal analysis (DTA).- 11.3 Differential scanning calorimetry (DSC).- 11.4 Thermomechanical analysis (TMA) and dynamic mechanical analysis (DMA).- 11.5 Pyrolysis — gas chromatography.- 12 Overall Analytical Procedures and Their Automation.- 12.1 Sampling and sample pretreatment.- 12.2 Examples of analytical problems and procedures.- 12.3 The automation of analytical procedures.- 13 The Role of Computers and Microprocessors in Analytical Chemistry.- 13.1 Introduction.- 13.2 Computers and microprocessors.- 13.3 Instrument-computer interfaces.- 13.4 The scope of microprocessor control and computers in analytical laboratories.

Su questa edizione

• Editore: Chapman & Hall
• Data di pubblicazione: 1995
• ISBN 10: 0751402265
• ISBN 13: 9780751402261
• Rilegatura: Copertina rigida
• Numero edizione: 4
• Numero di pagine: 560