Multistage separation processes are essentially the heart and soul of the petroleum, petrochemical, and chemical industries. They yield products as common as gasoline and plastics and those as specialized as medical-grade pharmaceuticals. Predicting the Performance of Multistage Separation Processes provides chemical engineers with solid information and insights into these processes. It reaches beyond fundamental principles to focus on intuitive understanding and practical interpretation. To that end, it presents numerous examples from a variety of applications, effectively demonstrating the performance of processes under varying conditions and the relationship among the different operating variables. With major advances in computational techniques for solving complex multistage separation equations, a variety of simulation programs have emerged that allow accurate and efficient prediction of multistage separation processes. These are valuable and effective tools, but are often hampered by a lack of understanding of the fundamentals and limitations of prediction techniques. The author addresses these problems and pursues a strategy that decouples the discussion of conceptual analysis and the computational techniques. Although Dr. Khoury presents mathematical methods in detail, he gives special attention to keeping the practical interpretation of the models in focus and emphasizes intuitive understanding. He applies graphical techniques and shortcut methods wherever possible and includes industrial practice heuristics about the ranges of operating variables that will work. With its updates and the addition of more than 100 new applications problems and solutions, Predicting the Performance of Multistage Separation Processes, Second Edition is ideal for a methodical study of separation processes and as a reference for the fundamental principles and shortcuts useful to the working professional.
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THERMODYNAMICS AND PHASE EQUILIBRIA. Thermodynamic Fundamentals. PVT Behavior of Fluids. Phase Equilibria. Enthalpy. THE EQUILIBRIUM STAGE. Phase Behavior. Performance of the Equilibrium Stage. Solution Methods. FUNDAMENTALS OF MULTISTAGE SEPARATION. Cascaded Stages. Distillation Basics. Absorption/Stripping Basics. MATERIAL BALANCES IN MULTCOMPONENT SEPARATION. Mathematical Model. Types of Column Specifications. BINARY DISTILLATION: PRINCIPLES. Column Section. Total Column. Column Solution with Mass and Enthalpy Balances. BINARY DISTILLATION: APPLICATIONS. Parameters Affecting Column Performance. Parameter Interactions in Fixed Configuration Columns. Design Strategies Guided by Graphical Representation. MULTICOMPONENT SEPARATION: CONVENTIONAL DISTILLATION. Characteristics of Multicomponent Separation. Factors Affecting Separation. Specifying Column Performance. Number of Trays and Feed Location. ABSORPTION AND STRIPPING. Thermal Effects. Liquid-to-Vapor Ratios. Number of Stages. Performance Specifications. Graphical Representation. COMPLEX DISTILLATION AND MULTIPLE COLUMN PROCESSES. Multiple Feeds. Multiple Products. Side Heaters/Coolers and Pumparounds. Multiple Column Processes. AZEOTROPIC AND EXTRACTIVE DISTILLATION: THREE-PHASE DISTILLATION. The Function of Entrainers and Solvents. Separation Processes. Three-Phase Distillation. LIQUID-LIQUID EXTRACTION. Extraction Fundamentals and Terminology. Graphical Representation. Extraction Equipment. SHORTCUT METHODS. Columns at Total Reflux. Minimum Reflux Ratio. Column Design and Performance Analysis. Modular Shortcut Methods. RIGOROUS METHODS
TRAY HYDRAULICS. General Tray Hydrdaulics Characteristics. Factors Affecting Tray Hydraulics. Flooding. Pressure Drop. Operable Ranges. Steps in Analysis of Tray Hydraulics. PACKED COLUMNS. Continuous Differential Mass Transfer. Rate of Mass Transfer. Mass Transfer in Packed Columns. General Packed Column Design. TRAY EFFICIENCY. Types of Tray Efficiency. Theoretical Model. Empirical Methods. BATCH DISTILLATION. Principles of Batch Distillation. Solution Methods. INDEX.
Book by Khoury Fouad M
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