100 And More Basic Nmr Experiments: A Practical Course - Brossura

Braun, Siegmar; Kalinowski, H.-O.; Berger, S.; Braun, S.; Kalinowski, Hans-Otto; Berger, Stefan

Brossura

ISBN 10: 3527290915 ISBN 13: 9783527290918

Casa editrice: Vch Pub, 1996

Riassunto

This practical course aims to enable the reader to understand the field of NMR experiments for structure determination. The experiments featured have been chosen mainly because of their importance and general applicability. Three compounds have been chosen as the main demonstration samples - chloroform, ethyl crotonate and strychnine (which should be used as a sealed sample). A scheme has been adopted for the detailed description of the experiments, organized in the following specific sections: "Purpose" explains the idea and goal of the experiment and refers the user to related experiments; "Literature" presents references to the original publication and to improvements and/or sections in monographs and reviews; "Pulse Scheme and Phase Cycle" gives the pulse sequence in an instrument-independent graphic and self-explanatory form, and the phase cycles of the pulses and the receiver; "Acquisition" is the main section, with instructions on the sample to be used, the spectrometer configuration, the type of programme and the parameters necessary for the performance of the experiment; "Processing" describes how to treat the time-domain data; "Results" presents the spectrum obtained by following the procedure exactly; and "Comments" contains an explanation of the most important steps of the pulse sequence. In general, the conditions for the experiments have not been optimized. In all cases, the results are presented exactly as they were obtained, without cosmetic retouching; sometimes, the samples used even show impurities.

Su questo libro

Recensione:

... an essential purchase for all NMR devotees ... honest, well focused and most adequately produced ... A wealth of information is clearly expressed and provided. Post–graduate students will find it of particular value.
Analyst

.. it is a marvelous and magnificent teaching book as well for beginners as for masters having to teach NMR. We like enormousy such manner to consider the learning of a new technique and we hope that many, if not all our readers will follow this new "Champs Elysées" or "Campus Elisearum", the pathway followed by gods in the greek mythology, but having become the daily highway of the scientists, who are, in some part, the followers of these gods, since they create all new stuff for the progress of the science.
Cellular and Molecular Biology

Product Description:

Book by Braun Siegmar Kalinowski HansOtto Berger Stefan

Su questa edizione

• Editore: Vch Pub
• Data di pubblicazione: 1996
• ISBN 10: 3527290915
• ISBN 13: 9783527290918
• Rilegatura: Copertina flessibile
• Numero di pagine: 418