High Resolution NMR in the Solid State: Fundamentals of CP/MAS

Stejskal, E. O.; Memory, J. D.

ISBN 10: 0195073800 / ISBN 13: 9780195073805

Editore: Oxford University Press, 1994

Riguardo questo articolo

With a black remainder mark, otherwise a fine, like new, hardcover first edition copy, slick pictorial binding, no DJ, black spine. Inscribed by Prof. Stejskal on the title page. Another fine product from NCSU.

Codice articolo 093136

Dati bibliografici

• Titolo: High Resolution NMR in the Solid State: Fundamentals of CP/MAS
• Editore: Oxford University Press
• Data di pubblicazione: 1994
• Lingua: Inglese
• ISBN 10: 0195073800
• ISBN 13: 9780195073805
• Rilegatura: Hardcover
• Edizione: First Edition
• Condizione: Fine
• Condizione della sovraccoperta: No DJ
• Firmato: Inscribed by Author(s)

Descrizione articolo

Riassunto

This text was developed from a course for physical chemistry and chemical physics students using cross-polarization (CP) magic angle spinning (MAS) NMR in their laboratory assignments. The book provides students with the details of the CP/MAS experiment as it is used to obtain rare-spin, high-resolution NMR spectra. The design of the CP/MAS experiments and the interpretation of spectra and relaxation measurements require an understanding of the interplay of several fundamental physical interactions not normally encountered in solution NMR. The student can observe the way interacting spin systems behave in the solid state, and have a quantum mechanically rigorous understanding of solid-state spin phenomena. The text will have the added benefit of serving as a self-study resource for students seeking to learn the underlying principles of laboratory experiments using the technique. The history of NMR is also treated, and the instrumentation of the spectrometer and probe are discussed.

Recensione

To say that the appearance of a book on the fundamentals of CP/MAS is timely would be a gross understatement ... this is an excellent book and should be read carefully, and understood, by all practitioners of CP/MAS NMT spectroscopy. (Glenn Penner, University of Guelph, Magnetic Resonance in Chemistry, Vol. 33 989 (1995))